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Selective Monoformylation Of 1,3-Diaminopropane Derivatives

 

作者: LilianaR. Orelli,   MaríaB. Garcia,   Fernando Niemevz,   IsabelA. Perillo,  

 

期刊: Synthetic Communications  （Taylor Available online 1999）
卷期: Volume 29, issue 11  

页码: 1819-1833

 

ISSN:0039-7911

 

年代: 1999

 

DOI:10.1080/00397919908086172

 

出版商: Taylor & Francis Group

 

数据来源: Taylor

 

摘要:

A general procedure for regiospecific construction ofN-aryl-N'-formyl-1,3-diaminopropanes 2 (R=H) by selective monoformylation ofN-(3-aminopropyl)arylamines 1 is described. Compounds 1 are readily obtained with high yields by aminolysis of 3-bromopropylamine hydrobromide with aromatic amines. The present synthetic strategy was extended to the synthesis of otherN-acyl-N-aryl-1,3 -diaminopropanes.

 

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