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Preparation and absolute stereochemistry of (−)-acenaphthenol

 

作者: Yulin Hu,   Herman Ziffer,   J. V. Sllverton,  

 

期刊: Canadian Journal of Chemistry  (NRC Available online 1989)
卷期: Volume 67, issue 1  

页码: 60-62

 

ISSN:0008-4042

 

年代: 1989

 

DOI:10.1139/v89-010

 

出版商: NRC Research Press

 

数据来源: NRC

 

摘要:

1-Acenaphthenol was resolved by fractional crystallization of its camphanate ester followed by hydrolysis. The absolute stereochemistry of the (+)-camphanate and (−)-alcohol, derived therefrom, was established as (R) by X-ray crystallography.Keywords: (−)-acenaphthenol, stereochemistry, synthesis, X-ray crystallography.

 

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