首页   按字顺浏览 期刊浏览 卷期浏览 Conditions Pertinent to the Occurrence of Fiber Orientation in Iron Films <1000 &Ari...
Conditions Pertinent to the Occurrence of Fiber Orientation in Iron Films <1000 Å Thick Deposited onto Amorphous Substrates

 

作者: Roger W. Clapp,  

 

期刊: Journal of Applied Physics  (AIP Available online 1962)
卷期: Volume 33, issue 8  

页码: 2539-2541

 

ISSN:0021-8979

 

年代: 1962

 

DOI:10.1063/1.1729013

 

出版商: AIP

 

数据来源: AIP

 

摘要:

Iron films having thicknesses of 20, 100, and 250 Å were deposited from the vapor in a vacuum of about 2×10−5mm Hg at a rate of deposition of approximately 8 Å/sec onto Formvar substrates initially at room temperature and onto silica substrates initially at 50°C. Prior to deposition the latter were baked‐out at 500°C for 1 h. Transmission electron diffraction patterns of the specimens were examined with a microphotometer and no evidence of fiber orientation was found. These experiments were repeated with films being deposited at pressures of 10−2and 10−1mm Hg of helium introduced into the system after initial evacuation of the system to about 2×10−5mm Hg. Again random orientation was observed for both the Formvar and silica‐backed films. Comparison of the conditions characterizing this work with those describing similar work in which a fiber texture did occur leads to the formulation of the hypothesis that if the experimental technique does not include at least one of two conditions (high deposition rate, high substrate/deposit surface temperature), then fiber orientation is not likely to occur in thin (<1000 Å) iron films deposited onto amorphous substrates, but only in thick films for which prolonged exposure to the radiant source eventually sufficiently elevates the surface temperature. A qualitative description of the processes involved is suggested.

 

点击下载:  PDF (248KB)



返 回