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Electron Probe and X-Ray Diffraction Microanalyses of Human Enamel Treatedin vitroby Fluoride Solution

 

作者: C.A. Baud,   S. Bang,  

 

期刊: Caries Research  (Karger Available online 1970)
卷期: Volume 4, issue 1  

页码: 1-13

 

ISSN:0008-6568

 

年代: 1970

 

DOI:10.1159/000259621

 

出版商: S. Karger AG

 

关键词: Enamel;Fluoride;Microanalysis

 

数据来源: Karger

 

摘要:

Fluoride uptake, topographic distribution, and effect on human dental enamel following topical treatment (for 4 min, 8 min and 72 h) with an acidulated fluoride-phosphate solution have been studied by means of electron probe X-ray microanalysis and X-ray diffraction. The samples examined were divided into a non-washed group, and a washed group from which excessive and loosely bound F had been eliminated from the enamel. The topographic distribution of fluorine was demonstrated by electron probe X-ray microanalysis. In the non-washed samples, an outer layer with a higher concentration of F, and adjacent to this another layer having a moderate concentration of F, were observed. After a prolonged washing about 90% of F of the outer layer was eliminated, whereas that of the inner layer persisted. X-ray diffraction analysis shows the presence of CaF2 in non-washed samples; the lines of CaF2 disappear after prolonged washing. On the other hand, a displacement of the apatite lines was observed in all treated samples, corresponding to a shortening of the parameter a of the unit cell, due to the replacement of the OH–– by F–– in the crystalline network. These results show that by topical treatment of enamel with an acidulated fluoride-phosphate solution, an accumulation of F in the surface layers of the enamel is produced, partly as CaF2 and partly as fluor

 

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