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Development of heating holders for the field-emission scanning electron microscope

 

作者: Youiti Yamamoto,   Kouji Higuchi,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1997)
卷期: Volume 68, issue 4  

页码: 1756-1758

 

ISSN:0034-6748

 

年代: 1997

 

DOI:10.1063/1.1147987

 

出版商: AIP

 

数据来源: AIP

 

摘要:

We have developed a practical heating holder for the field-emission scanning electron microscope (FESEM, JSM-6000F) to study and apply the specimen heated and electron beam induced conductivity. The design is described in detail. A surface temperature up to 943 K is achieved. The temperature fluctuation is less than 0.5&percent;/h at about 20 min after the heating up to 943 K, and the thermal drift is suppressed to less than 5 nm/min up to 873 K. The temperature of the observation area is proportional to the input power of the heater up to about 700 K. The charging on a nonconducting surface such as porous pipe glass can be prevented at a surface temperature above about 673 K. It is demonstrated that this is useful to the high resolution observations of the nonconducting surfaces. ©1997 American Institute of Physics.

 

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