Retrograde Densification of Calcined and Glass Precursors of Approximate (Bi,Pb)2Sr2Ca2Cu3O10Stoichiometry
作者:
Dimitri N. Argyriou,
Eric R. Vance,
期刊:
Journal of the American Ceramic Society
(WILEY Available online 1992)
卷期:
Volume 75,
issue 5
页码: 1269-1271
ISSN:0002-7820
年代: 1992
DOI:10.1111/j.1151-2916.1992.tb05568.x
出版商: Blackwell Publishing Ltd
关键词: densification;superconductors;kinetics;glass;high temperature
数据来源: WILEY
摘要:
Retrograde densification of pelletized calcines and glasses having an approximate (Bi,Pb)2Sr2Ca2Cu3O10starting stoichiometry and sintered at ∼850°C can be described by first‐order rate equations. Retrograde densification in the calcine precursors was largely due to the development of open pores, and was approximately proportional to the concentration of the (Bi,Pb)2Sr2CaCu3O10phase. In the glasses, retrograde densification is mainly caused by porosity accompanying the growth of a needlelike Sr─Ca─Cu─O phase, together with (Bi,Pb)2Sr2Ca2Cu3O10and (Bi,Pb)2
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