A Direct and Sensitive Method for the Determination of Salicylamide in Microplasma Samples by High-Performance Liquid Chromatography Using Fluorescence Detection
作者:
S.R. Gautam,
V. Chungi,
A. Hussain,
S. Babhair,
D. Papadimitrou,
期刊:
Analytical Letters
(Taylor Available online 1981)
卷期:
Volume 14,
issue 8
页码: 577-582
ISSN:0003-2719
年代: 1981
DOI:10.1080/00032718108055471
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A quantitative analysis of salicylamide in microplasma volumes by high-performance 1iquid chromatography using fluorescence detection is reported. The procedure is extremely simple and very rapid, involving the direct introduction of the plasma sample on the HPLC column. The assay procedure is linear over the concentration range studied, 0–100 ng/ml with correlation coefficient for the linear regression, r = 0.998. This assay procedure enables the detection of salicylamide as low as 5.0 ng/ml in plasma, using sample volume of 100 μl.
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