Procedure for loading diamond cells with high‐pressure gas
作者:
R. L. Mills,
D. H. Liebenberg,
J. C. Bronson,
L. C. Schmidt,
期刊:
Review of Scientific Instruments
(AIP Available online 1980)
卷期:
Volume 51,
issue 7
页码: 891-895
ISSN:0034-6748
年代: 1980
DOI:10.1063/1.1136333
出版商: AIP
数据来源: AIP
摘要:
We devised an apparatus and technique for loading diamond‐anvil cells with gases at high pressure. Cells were filled quickly and conveniently at room temperature with helium and hydrogen isotopes to initial densities exceeding those of the normal liquids. We report preliminary values of4He and D2melting points based on the ruby pressure scale and compare them with extrapolations from our earlier melting curves measured to 20 kbar in a piston‐cylinder device. Our filling procedure now makes it possible to use4He as a pressure medium in diamond cells. The technique is also useful for loading cells with gaseous mixtures.
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