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Improved oscillating buoy viscometer

 

作者: Rogers C. Ritter,   Janelle A. Molloy,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1987)
卷期: Volume 58, issue 12  

页码: 2306-2312

 

ISSN:0034-6748

 

年代: 1987

 

DOI:10.1063/1.1139342

 

出版商: AIP

 

数据来源: AIP

 

摘要:

An improved design of the vertically oscillating buoy viscometer with real‐time computer control, evaluation, and plotting is presented. In this method, the optically observed phase lag of the buoy relative to a sinusoidal driving force is a direct and absolute measure of viscosity. Construction features of the new version improve reassembly precision and give three‐axis positioning of the sphere, as well as an 80‐fold improvement in the signal‐to‐noise ratio for small amplitudes of the buoy motion. Design of the ‘‘crossed coil’’ system is discussed and the magnetic and mechanical faults which lead to various kinds of motional instability are considered. Boundary layer corrections are now computer corrected as are temperature variations. The evaluation of ‘‘intrinsic viscosity’’ as a measure of molecular ellipticity is discussed and one measurement set is presented.

 

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