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Reaction of (t‐BuGaCl2)2with Ar′PHLi (Ar′ = 2,4,6‐t‐Bu3C6H2): Preparation of the chloride‐bridged dimer (t‐BuGa(Cl)P(H)Ar′)2

 

作者: Alan H. Cowley,   Richard A. Jones,   Miguel A. Mardones,   Jerry L. Atwood,   Simon G. Bott,  

 

期刊: Heteroatom Chemistry  （WILEY Available online 1991）
卷期: Volume 2, issue 1  

页码: 11-15

 

ISSN:1042-7163

 

年代: 1991

 

DOI:10.1002/hc.520020103

 

出版商: VCH Publishers, Inc.

 

数据来源: WILEY

 

摘要:

AbstractThe reaction of (t‐BuGaCl2)2with Ar′P(H)Li (AR′ = 2,4,6‐t‐Bu3C6H2) affords the chloride‐bridged dimer [t‐BuGa(Cl)P(H)Ar′]2(1). The structure of1has been established by X‐ray crystallography. Compound1, C44H78Cl2Ga2P2, crystallizes in the monoclinic space group P21/n withZ= 2, a = 10.468(1), b = 14.967(1), c = 16.182(2) Å, and Å = 94.48(1)β. The reaction of1wit

 

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