Preparation of Surface Standards of Copper on Substrates of Platinum and Glass for X-Ray Photoelectron Spectroscopy in Adsorption Studies
作者:
C.S. P. Iyer,
H.W. Nürnberg,
H.J. Krebs,
期刊:
Analytical Letters
(Taylor Available online 1985)
卷期:
Volume 18,
issue 4
页码: 519-527
ISSN:0003-2719
年代: 1985
DOI:10.1080/00032718508066151
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
Changes in concentration of very dilute solutions of metals, due to adsorption on the walls of the container, are well known. Earlier studies, however, have been confined to follow the changes in trace metal concentration of the solution phase with time. Characterisation of the solid surface is equally important and for such a study are needed reproducible thin layers of the ions under consideration on the particular substrate. Deposition of thin layers of copper on platinum by electrodeposition and solution evaporation of CuCl2on platinum gave comparable results on examination of the Cu 2p peaks by XPS. Solution evaporation was found successfully for the sodium glass substrate as well. However, solution evaporation could not be applied to Teflon or PVC substrates.
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