Phosphorus-Containing Nadimide Resins: Synthesis and Characterization
作者:
I.K. Varma,
H.P. Mittal,
期刊:
Journal of Macromolecular Science: Part A - Chemistry
(Taylor Available online 1989)
卷期:
Volume 26,
issue 7
页码: 937-950
ISSN:0022-233X
年代: 1989
DOI:10.1080/00222338908052022
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A series of phosphorus-containing nadimide-endcapped resins was prepared by reactingendo-5-norbornene-2,3-dicarboxylic acid anhydride (nadic anhydride), 3,3′,4,4′-benzophenonetetracarboxylic acid dian-hydride, and tris(3-aminophenyl)phosphine oxide in glacial acetic acid/ dimethylformamide. Structural characterization of resins was done by elemental analysis, FTIR, and1H NMR. In DSC traces of these resins, an exothermic transition associated with crosslinking was observed above 280°C. Thermogravimetrie studies revealed a multistep decomposition reaction. Residual weight at 800°C in nitrogen was found to depend on the backbone structure and ranged from 42 to 60%.
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