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Synthesis of 8,3′-Thioanhydroguanosine

 

作者: Kelvin K. Ogilvie,   Lewis A. Slotin,   Denis C. K. Lin,   John B. Westmore,  

 

期刊: Canadian Journal of Chemistry  （NRC Available online 1972）
卷期: Volume 50, issue 20  

页码: 3276-3279

 

ISSN:0008-4042

 

年代: 1972

 

DOI:10.1139/v72-524

 

出版商: NRC Research Press

 

数据来源: NRC

 

摘要:

The synthesis of 8,3′-thioanhydroguanosine is described. The anhydro ring is formed by displacement of bromine from position-8 and methanesulfonate from the 3′-position using thiourea in refluxingn-butanol. The 8,3′-thioanhydroguanosine is converted by Raney nickel reduction to 3′-deoxyguanosine, an analogue of cordycepin.

 

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