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Spectrographic Determination of Eleven Trace Impurities in High Purity Cadmium

 

作者: P.S. Murty,   V.H. P. Kaimal,  

 

期刊: Analytical Letters  (Taylor Available online 1979)
卷期: Volume 12, issue 12  

页码: 1249-1258

 

ISSN:0003-2719

 

年代: 1979

 

DOI:10.1080/00032717908067915

 

出版商: Taylor & Francis Group

 

关键词: Cadmium;Spectrographic analysis.

 

数据来源: Taylor

 

摘要:

Eleven trace impurities are determined in high purity cadmium by employing d. c. arc emission spectrographic technique. Cadmium ie converted t o its oxide and ground with high purity conducting graphite powder which acts as a buffer. Forty milligrammes of the above mixture is excited in a d. c. arc set at 12 amperes. The spectra of the sample and synthetic standards are photographed on a Jarrell-Ash 3.4 meter Ebert plane grating spectrograph in the region 2175 - 3425 A using a 1200 lines per mm grating in the first order. The detection limits obtained range from 1 to 10 ppm for different elements. The average coefficient of variation ranges from 8.0 to 15.7% for the impurities.

 

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