High Temperature Mass Spectrometer Sample System
作者:
H. M. Shin,
H. K. Hahm,
S. I. Kwon,
S. H. Jo,
S. B. Hong,
期刊:
Review of Scientific Instruments
(AIP Available online 1960)
卷期:
Volume 31,
issue 11
页码: 1200-1202
ISSN:0034-6748
年代: 1960
DOI:10.1063/1.1716851
出版商: AIP
数据来源: AIP
摘要:
A General Electric analytical mass spectrometer, which was originally designed only for gaseous samples, has been modified so that the sample system can be converted for application to solid samples at elevated temperatures up to 1000°C. Conversion is accomplished by the complete replacement of the sample system by a magnetically operated device and a cavity furnace, the heater of which is thermally attached to the furnace body and servo‐controlled to keep to the predetermined temperature within a fraction of a degree. The furnace body is a silica tube, 5 mm i.d. Replacement of the sample can be done within 10 min without breaking the major vacuum. Advantages and disadvantages compared to the Knudsen cell are also discussed.
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