A number of metal-furazolidone complexes have been synthesized and screened for antibacterial and antifungal activity. The study reveals the remarkable efficacy of Co(II), Cu(II), Zn(II) and Cd(II) complexes against the various strains of bacteria and fungi, viz.,Pseudomonas mangiferae, Bacillus pumillus, andSalmonella typhisuggest a strong possibility of its application for the treatment of fungal skin infections. The most striking feature has been the activity of Cu-furazolidone complex, it was found to be uniformly active against all the strains of bacteria and fungi under study. Electroanalytical findings of these metal furazolidone complexes have also been performed.