Measurement of 3,4 Dihydroxyphenyl Ethylene Glycol (DOPEG) in Plasma by High Performance Liquid Chromatography with Electrochemical Detection
作者:
C. Cann-Moisan,
J. Caroff,
P.Le Bras,
E. Girin,
O. Curet,
J.M. Gandon,
期刊:
Journal of Liquid Chromatography & Related Technologies
(Taylor Available online 1996)
卷期:
Volume 19,
issue 19
页码: 3119-3124
ISSN:1082-6076
年代: 1996
DOI:10.1080/10826079608015811
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
Usually, determination of DOPEG in plasma by EC-HPLC is always performed after extraction on alumina. This paper presents an extraction on boric acid gel, with good selectivity, reproducibility. In high sensitivity conditions (0.5 nA full scale) an autosampler is used and presents two major advantages: first, the possibility of storing samples in cold conditions to preserve stability of DOPEG, second the analysis of numerous samples in pharmacological studies, for example.
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