Improved TLC systems for rapid resolution of phenyl thiohydantoin amino acids
作者:
R. Bhushan,
V. K. Mahesh,
P. V. Mallikharjun,
期刊:
Biomedical Chromatography
(WILEY Available online 1989)
卷期:
Volume 3,
issue 1
页码: 43-45
ISSN:0269-3879
年代: 1989
DOI:10.1002/bmc.1130030111
出版商: John Wiley&Sons, Ltd.
数据来源: WILEY
摘要:
AbstractTwo new solvent systems, n‐hexane + propionic acid (26:5, v/v) and chloroform + acetone (29:3, v/v), for the rapid resolution and identification of an 18‐component mixture of phenylthiohydantoin amino acids are reported. Using these systems certain difficult combinations of phenylthiohydantoin amino acids are resolved. Two more solvent systems, viz chloroform+acetic acid (27:3, v/v) and chloroform + methanol (30:4, v/v), are developed to resolve phenylthiodantoin derivatives of aspartic and glutamic ac
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