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Quasiequilibrium determination of high‐Tcsuperconductor transition temperatures

 

作者: Michael J. Pechan,   Jonathan A. Horvath,  

 

期刊: American Journal of Physics  (AIP Available online 1990)
卷期: Volume 58, issue 7  

页码: 642-644

 

ISSN:0002-9505

 

年代: 1990

 

DOI:10.1119/1.16424

 

出版商: American Association of Physics Teachers

 

关键词: TRANSITION TEMPERATURE;ACCURACY;YTTRIUM OXIDES;BARIUM OXIDES;COPPER OXIDES;BENCH−SCALE EXPERIMENTS;LOW TEMPERATURE;NITROGEN;SUPERCONDUCTORS

 

数据来源: AIP

 

摘要:

A fast and inexpensive method for making accurate determinations of transition temperatures above 77 K in superconducting oxides is presented. The technique is based upon cooling in liquid nitrogen, then warming the sample in the vapors above the liquid level inside a standard glass or stainless steel vacuum bottle. Proper sample support and placement of the thermocouple, key elements in this technique, are discussed. Once pads have been placed on the sample,Tccan be determined, to an accuracy of ±1 K, within 15 min. Due to its speed, accuracy, and low cost, this technique is well suited for application in an advanced undergraduate laboratory experiment.

 

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