The shear creep and recovery behavior of narrow molecular weight atactic polystyrene (APS) (6.7×105Mw) solutions (27.3 wt. %) in two solvents (n‐amyl andn‐butyl acetate) were studied at various temperatures down to −83 °C above and below reported thermoreversible gel points (∼−50 °C). In both cases viscous flow was measured above and below the reported gel points. The resulting compliance curves for two solutions (n‐amyl andn‐butyl acetates) were successfully reduced toT0=−82 and −61 °C, respectively, indicating viscoelastic liquid response down to −82 °C. These solutions were clear. A solution of 18.7% APS (3.9×105Mw) in iso‐amyl acetate was also studied. It responded similarly to the first solutions untilT=−49 °C when it became cloudy, indicating phase separation. At lower temperatures the viscosity increased dramatically, suggesting gel‐like behavior.