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The Carbon-13 Magnetic Resonance Spectrum of an Organic Peroxide

 

作者: A.Harry Andrist,   MarkJ. Kovelan,  

 

期刊: Spectroscopy Letters  （Taylor Available online 1975）
卷期: Volume 8, issue 8  

页码: 547-550

 

ISSN:0038-7010

 

年代: 1975

 

DOI:10.1080/00387017508067358

 

出版商: Taylor & Francis Group

 

关键词: β,β'-Dimethoxyperoxide;Cmr Spectrum

 

数据来源: Taylor

 

摘要:

Phenanthrene ozonide and methanol combine under acid catalysis to produce a 1:1 adduct, mp 180–181°, assigned structure1on the basis of C-H analysis and infrared spectrum.1,2Although β,β′-dihydroxyalkylperoxides have been isolated from equilibrium mixtures of aldehydes and hydrogen peroxide, they are rarely if ever as thermally stable as the phenanthrene ozonide:methanol adduct.3

 

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