Ion implantation allows controlled introduction of impurities into diamond. A basic problem is to determine if the implanted layers are dominated by substitutional doping or radiation damage effects. Optical and electrical measurements on the implanted diamonds revealed (1) a degradation of the band-gap and sample coloration, (2) no optical absorption levels which would be characteristic of hydrogenic ionization levels, (3) resistivity activation energies of 0.2 to 0.3 eV independent of the ion specie, and (4) no measurable Hall Effect.