Equipment news

 

作者:

 

期刊: Analytical Proceedings  (RSC Available online 1982)
卷期: Volume 19, issue 1  

页码: 46-50

 

ISSN:0144-557X

 

年代: 1982

 

DOI:10.1039/AP9821900046

 

出版商: RSC

 

数据来源: RSC

 

摘要:

46 EQUIPMENT NEWS Artal. PYOC, Equipment News Further details of all items reported below are available from the companies concerned. For rapid information please complete the Reader Enquiry Service card (circle the appropriate number mentioned), rather than approaching companies direct. Conductivity Meter The CDM83 measures conductivity from 1300 pS cm-l to 1300 mS cm-l full scale, with auto- matic switching to the optimal range and frequency. Temperature correction to a refer- ence temperature and full adjustment of the cell constant are provided. In addition to conductivity, the 20-character alphanumeric display may simultaneously show sample or reference temperature from - 10.0 "C to + 105.0 OC, or temperature coefficient or cell constant. Radiometer A/S. Circle 510. GC - MS Column for Drug Analysis The HP59858 GC - LC - MS fused silica system permits the separation of acidic and basic drugs on a single column.Hewlett Packard Ltd. Circle 511. Electrophoresis Power Supply The Model 500/200 has a range of 0-500 V and 0-200 mA; either parameter can be set to a constant level. Overload protection is provided. Bio-Rad Laboratories Ltd. Circle 5 12. Photoacoustic Cell The Model 410.10 has been designed for use in Fourier transform infrared and laser-based systems. The cell accepts samples up to 6 mm in diameter by 2 mm thick and entrance windows are interchangeable. A power-supply and pre-amplifier with 1OOx gain and 20 kHz band width are provided. EDT Research. Circle 513. Cryo-microtome The Cryo-Cut I1 incorporates the Spencer rotary microtome, fast-feed control, automatic de-frost cycle and quick-freeze facility. Reichert- Jung UK.Circle 514. Filters for Liquid Chromatography The SSI pump inlet type is rated at lOpm, surface area 7.7 cm2 and total internal volume 1150 p1. The high pressure line type is rated at 0.5 pm, 2.5 cm2 and 580 pl. The element is corrosion resistant. Scientific Glass Engineering (UK) Ltd. Circle 51 5. Laser Ion Mass Analyser This analyser measures the concentrations at the p.p.m. level of elements in the relative46 EQUIPMENT NEWS Artal. PYOC, Equipment News Further details of all items reported below are available from the companies concerned. For rapid information please complete the Reader Enquiry Service card (circle the appropriate number mentioned), rather than approaching companies direct.Conductivity Meter The CDM83 measures conductivity from 1300 pS cm-l to 1300 mS cm-l full scale, with auto- matic switching to the optimal range and frequency. Temperature correction to a refer- ence temperature and full adjustment of the cell constant are provided. In addition to conductivity, the 20-character alphanumeric display may simultaneously show sample or reference temperature from - 10.0 "C to + 105.0 OC, or temperature coefficient or cell constant. Radiometer A/S. Circle 510. GC - MS Column for Drug Analysis The HP59858 GC - LC - MS fused silica system permits the separation of acidic and basic drugs on a single column. Hewlett Packard Ltd. Circle 511. Electrophoresis Power Supply The Model 500/200 has a range of 0-500 V and 0-200 mA; either parameter can be set to a constant level.Overload protection is provided. Bio-Rad Laboratories Ltd. Circle 5 12. Photoacoustic Cell The Model 410.10 has been designed for use in Fourier transform infrared and laser-based systems. The cell accepts samples up to 6 mm in diameter by 2 mm thick and entrance windows are interchangeable. A power-supply and pre-amplifier with 1OOx gain and 20 kHz band width are provided. EDT Research. Circle 513. Cryo-microtome The Cryo-Cut I1 incorporates the Spencer rotary microtome, fast-feed control, automatic de-frost cycle and quick-freeze facility. Reichert- Jung UK. Circle 514. Filters for Liquid Chromatography The SSI pump inlet type is rated at lOpm, surface area 7.7 cm2 and total internal volume 1150 p1.The high pressure line type is rated at 0.5 pm, 2.5 cm2 and 580 pl. The element is corrosion resistant. Scientific Glass Engineering (UK) Ltd. Circle 51 5. Laser Ion Mass Analyser This analyser measures the concentrations at the p.p.m. level of elements in the relative48 ANALYTICAL PROCEEDINGS January, 1982 Analytical Sciences Monographs No. 4 Electrothermal Atomisation for Atomic Absorption Spectrometry by C. W. Fuller Since the introduction of atomic absorption spectrometry as an analytical technique, by Walsh, in 1953, the use of alternative atomization sources to the flame has been explored. At the present time the two most successful alternatives appear to be the electrothermal atomiser and the inductively- coupled plasma. In this book an attempt has been made to provide the author's views on the historical development, commercial design features, theory, practical considerations, analytical parameters of the elements, and areas of application of the first of these two techniques, electrothermal atomisation. Hardcover 135pp 0 85186 777 4 fl8.00 ($38.00) RSC Members fl3.50 No. 5 Dithizone by H.M. N. H. Irving The author of this monograph, who has been closely associated with the development of analytical techniques using this reagent for man! years, and who has made extensive investigations into the properties of its complexes, has gathered together a body of historical and technical data that will be of interest to many practising analytical chemists. Hardcover 112pp 0 85186 787 1 f12.50 ($27.00) RSC Members f9.50 No.6 lsoenzyme Analysis Edited by D. W. Moss This monograph attempts to draw together the most important experimental techniques which have resulted from the modern recognition that enzymes frequently exist in multiple molecular forms. This monograph also indicates the advantages and limitations in isoenzyme studies of these modern experiments. Brief Contents: Multiple Forms of Enzymes; Separation of Multiple Forms of Enzymes; Selective Inactivation of Multiple Forms of Enzymes; lmmunochemistry of Multiple Forms of Enzymes; Catalytic Differences between Multiple Forms of Enzymes, Methods of Obtaining Structural Information, Selection of Methods of Analysis. Hardcover 171pp 0 85186 800 2 f12.00 ($26.00) RSC Members f9.00 No. 7 Analysis of Airborne Pollutants in Working Atmospheres The Welding and Surface Coatings Industries by J.Moreton and N. A. R. Falla This Monograph covers the following: Part I The Welding Industry: Airborne Pollutants in Welding; Sampling of Welding Workshop Atmospheres; Analysis of Welding Fumes and Pollutant Gases. Part II The Surface Coatings Industry: Origin of Airborne Pollutants in the Surface Coatings Industry; Collection and Analysis of Gaseous Atmospheric Pollutants in the Surface Coatings Industry; Collection and Analysis of Particulate Atmospheric Pollutants in the Surface Coatings Industry; Future Trends Relating to Sampling and Analysis in the Welding and Surface Coatings Industries. Hardcover 192pp 0 85186 860 6 f15.00($32.00) RSC Members f12.00 No. 8 The Sampling of Bulk Materials by R.Smith and G. V. James The literature of analytical chemistry exhaustively covers the many techniques now available to the analyst. feature common to a l l analyses, is in contrast only sparsely documented. Comparatively few original papers on this subject have been published in the last fifty years; there are very few reviews available, and perhaps as a result sampling is badly neglected in most instructional courses in analytical chemistry. This Monograph will go some way towards filling a gap in the literature and should stimulate interest in the development of sampling as a field of study. Brief Contents Introduction; Glossary of Terms; Establishment of a Ssmpling Scheme; Sampling Theories; Apparatus for Sam2ling; Sampling Methods; Appendices 1-4.Hardcover 200pp 0 851 86 81 0 X f16.50 ($35.00) RSC Members f10.75 Orders: RSC Members should send their orders to: The Membership Officer, The Royal Society of Chemistry, 30 Russell Square, London WC1B 5DT All other orders should be Sent to: The Royal Society of Chemistry, Distribution Centre, Blackhorse Road, Letchworth. Herts. SG6 1 HN Sampling, the one The Royal Society of ChemistryJanuary, 1982 ANALYTICAL PROCEEDINGS 49 RSC Publications S PEClALlST PER 10 DICAL R EPO RTS Nuclear Magnetic Resonance Vol. 10 Senior Reporter: G. A. Webb A review of the literature published between June 1979 and May 1980. Brief Contents : Theoretical and Physical Aspects of Nuclear Shielding; Applications of Nuclear Shielding; Theoretical Aspects of spin-spin couplings; Applications of spin-spin couplings; Nuclear Spin Relaxation Fluids; Solid State N.M.R.; Multiple Resonance; Natural Macromolecules; Synthetic Macromolecules; Conformational Analysis; N.M.R.of Paramagnetic Molecules; N.M.R. of Liquid Crystals and Micellar Solutions; "A subject index at the end, many tables and a clear table of contents at the beginning of each chapter complete this volume, which ought to be present in all university chemistry libraries." European Spectroscopy News, reviewing Vol. 8 Hardcover 372pp 0 851 86 332 9 Price f 51 .OO ($1 09.00) Photochemistry Vol. 11 Senior Reporter: D. Bryce-Smith This volume is the eleventh in the series of reviews in the field of phDtochemistry and covers the literature published between July 1978 and June 1979.Brief Contents : Part I : Physical Aspects of Photochemistry; Part I I : Photochemistry of Inorganic and Organometallic Compounds; Part II I; Organic Aspects of Photochemistry; Part IV: Polymer Photochemistry; Part V: Photochemical Aspects of Solar Energy Conversion; Part VI: Chemical Aspects of Photobiology. "All Chemistry libraries which have at least a pretence of completeness should have a copy of this volume and a standing order for future volumes in the series. The quality of the printing, reproduction of figures, and the paper itself is excellent, which is refreshing in these days of shortcuts and photoreplication. The senior reporter and his colleagues are to be congratulated on a demanding assignment in which a very high standard of performance has been set and consistently achieved".- Journal of Medicinal Chemistry, reviewing Vol. 8 Hardcover 704pp 0 85186 095 8 Price f70.00 ($149.00) Annual Reports On the Progress of Chemistry Vol.77 Annual Reports provides for the general reader critical coverage of the significant advances in the major areas of chemistry on an annual basis. From 1980, Section A became devoted solely to inorganic chemistry and therefore exhibited enhanced coverage of this area compared with previous years. Section C, a new Annual Reports volume on physical chemistry has been introduced which consists of authoritative critical accounts of progress in major areas by acknowledged experts. Section B covers organic chemistry. Vol. 77 1980 (to be published in Autumn 1981 ) Section A Inorganic Chemistry f 36.50 ($90.50) Section B Organic Chemistry f40.50 ($1 00.00) Section C Physical Chemistry f36.50 ($90.50) Orders should be sent to: Distribution Centre, Chemistry The Royal Society of The Royal Society of Chemistry, Blackhorse Road, Letchworth, Herts.SG6 1 HNAnal. PYOC. 50 ANALYTICAL CHEMISTRY TRUST FUND atomic mass range 1-500, e-g., hydrogen, in micron sized areas of bulk samples (e.g., welds), within a time of 1OOpS. A 20ns energy pulse from a laser is focused on to a 5pm spot on the sample. About 10pm3 of sample is vapourised, the ions extracted, accelerated and directed into a time of flight mass analyser. The ions are detected by an electron multiplier and the output is displayed on a storage oscilloscope and held in a transient recorder.Cambridge Consultants Ltd. Circle 516. PID Controller The Lauda R25 is suitable for use with platinum resistance thermometers and is compatible with Lauda thermostats with relay units R2 and R3 to give accuracies as high as f0.005 "C. It may be used as a proportional or on/off con- troller. Roth Scientific Co. Ltd. Circle 517. Rotating Disc Electrode The E628 can be equipped with a variety of interchangeable electrode tips for analysis and work on the kinetics of electrode reactions. Electronic control and stabilising circuits are incorporated. Two speeds are available, one for measurement and one for regeneration by polishing. can be. chosen over a wide range. Any desired number of revolutions Roth Scientific Co. Ltd. Circle 518. Software for Microprocessor -controlled Titrator A new software package extends the capabilities of the Titroprocessor. Additional parameters (set by the operator) include the quality of the end-point, so that significant inflections can be selected, an end-point window, for investigation of part of a curve, the identification of equi- valence points and a volume read-out for end- point titration. There is also the ability to work with one of two different burettes and two electrode chains. Roth Scientific Co. Ltd. Circle 519. Flow Cell for Spectrophotometry A sipper system for the DU-8 ultraviolet - visible spectrophotometer has been introduced. It consists of a temperature-controlled 8O-pl flow cell, a peristaltic pump and plug-in soft- ware (Compuset). The system provides fast and accurate measurement of concentration or rate results by comparison with a stored standard curve. The temperature (from 10 to 50 "C) is controlled with a precision of 0.05 "C. Beckman-RIIC Ltd. Circle 520.

 

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