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High‐Temperature Pressure‐Vacuum Furnace

 

作者: William Lodding,   Laurence Hammell,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1959)
卷期: Volume 30, issue 10  

页码: 885-886

 

ISSN:0034-6748

 

年代: 1959

 

DOI:10.1063/1.1716372

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A simple high‐temperature pressure‐vacuum furnace using a recrystallized alumina tube as the vessel with external resistance windings is described. Temperatures to 1900°C can be used in both strongly reducing and oxidizing atmospheres. Pressures to 28 atoms at 1200°C were obtained and no water cooling was required. Differential thermal analysis with continuous gas analysis of reaction products is made possible.

 

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