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High‐temperature ovens (1700 °C) for a wide range of oxygen gas pressures (10−6–2×103bar): A new two‐chamber autoclave

 

作者: J.‐Y. Genoud,   T. Graf,   G. Triscone,   A. Naula,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1994)
卷期: Volume 65, issue 12  

页码: 3829-3833

 

ISSN:0034-6748

 

年代: 1994

 

DOI:10.1063/1.1145215

 

出版商: AIP

 

数据来源: AIP

 

摘要:

We describe the construction of four different systems used for annealing samples in oxygen. The gas pressure can be controlled over nine decades (10−6–2×103bar). The maximum temperature, 1700 °C, is limited by the ceramic materials used for thermal insulation and for the crucibles. The low‐pressure furnaces (10−6–1 bar) have an external heating system and incorporate an active regulation of a small gas flow. The intermediate pressure furnaces (1–150 bar) are heated either by a special resistive wire or by rf heating with a Pt‐20%Rh susceptor, both in the pressurized gas chamber. Quenching is possible in the latter. For the kbar range, we designed a double‐chamber autoclave with separate heater and sample spaces, filled with Ar and O2. The gas pressures are balanced in a cold, separate vessel by means of a silicon hose. The temperature is measured with a thermocouple feeding into the hot, pressurized oxygen environment very close to the sample. The construction problems of this new autoclave have been solved with particular emphasis on the safety requirements. ©1994 American Institute of Physics.

 

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