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X‐Ray Diffraction Measurement of Strain in Multiphase Systems

 

作者: P. Cucka,  

 

期刊: Journal of Applied Physics  (AIP Available online 1967)
卷期: Volume 38, issue 10  

页码: 3959-3964

 

ISSN:0021-8979

 

年代: 1967

 

DOI:10.1063/1.1709047

 

出版商: AIP

 

数据来源: AIP

 

摘要:

It is shown that failure to take into account the nonuniformity of stress in particles near a surface may lead to gross errors when stress measurements are made by x‐ray diffraction on crystallites of one phase dispersed in a matrix of another phase. In particular, the measured strains may depend on the wavelength of the radiation used, and on the particle size of the dispersed phase even though the actual strains in particles not too close to the surface are not dependent on particle size. The measured strains may differ by a factor of two or three from the strains in particles below the x‐ray penetration depth. Experimental evidence on a vitreous china (quartz—glass) system is presented, showing that the observed variation of strain with wavelength and particle size is of about the magnitude predicted by calculation on a simple model system.

 

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