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Synthesis of [methoxy‐14C]eugenol

 

作者: Joseph E. Rice,   Nalband Hussain,   Edmond J. Lavoie,  

 

期刊: Journal of Labelled Compounds and Radiopharmaceuticals  （WILEY Available online 1987）
卷期: Volume 24, issue 9  

页码: 1043-1049

 

ISSN:0362-4803

 

年代: 1987

 

DOI:10.1002/jlcr.2580240905

 

出版商: John Wiley&Sons, Ltd.

 

关键词: Eugenol;Synthesis;Carbon‐14

 

数据来源: WILEY

 

摘要:

AbstractA short, efficient synthesis for [methoxy‐14C]eugenol from unlabelled eugenol is described. The free phenolic group is protected as a methanesulfonate ester prior to removal of the methoxyl group. Reaction of the resulting phenolic mesylate with [14C]methyl iodide under basic conditions followed by treatment with warm sodium hydroxide gave the title compound in good overall yiel

 

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