SODIUM BOROHYDRIDE AND HYDROGEN PEROXIDE AS FLUOROGENIC SPRAY REAGENTS FOR THE DETECTION OF NALIDIXIC ACID AND FLUMEQUINE
作者:
Mei-Lin Wang,
Sheng-Chih Chen,
Sheng-Chu Kuo,
期刊:
Journal of Liquid Chromatography & Related Technologies
(Taylor Available online 1999)
卷期:
Volume 22,
issue 5
页码: 771-775
ISSN:1082-6076
年代: 1999
DOI:10.1081/JLC-100101698
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A simple, sensitive and highly selective detection method for nalidixic acid and flumequine has been developed. A 1-μL aliquot of sample solution was spotted onto the thin-layer plate with the aid of a disposable micropipette, and after development, the plate was sprayed first with sodium borohydride and then hydrogen peroxide successively. The spots were visualized under longwave UV light. The detection limits were 30 pmol for nalidixic acid and 60 pmol for flumequine.
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