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Automatic Recording Vacuum Microbalance

 

作者: C. Norman Cochran,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1958)
卷期: Volume 29, issue 12  

页码: 1135-1138

 

ISSN:0034-6748

 

年代: 1958

 

DOI:10.1063/1.1716097

 

出版商: AIP

 

数据来源: AIP

 

摘要:

An automatic control and recording system for the null‐type vacuum microbalance of Czanderna and Honig [Anal. Chem29, 1206 (1957)] has been assembled from commercial components. A variable permeance transducer is employed to detect beam movement and to control a force to restore the beam to the null position. This force is recorded in a selection of ranges extending from 0–20 000 &mgr;g to 0–5 &mgr;g with accuracies ranging from 0.1% to 2% of full scale. On the most sensitive settings the balance can detect weight changes as small as 0.01 &mgr;g in loads up to 1 g. Stabilities of 0.1 &mgr;g have been observed for periods of many hours on the most sensitive ranges. The balance is undamped, and no corrections are made to the restoring force if beam oscillation is centered about the null point.

 

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