Stopped-Flow Spectrophotometric Determination of Dopamine and Methyldopa with Sodium Hydroxide.
作者:
JuanJ. Berzas,
JoséM. Lemus,
Prado Buitrago,
期刊:
Analytical Letters
(Taylor Available online 1997)
卷期:
Volume 30,
issue 6
页码: 1109-1120
ISSN:0003-2719
年代: 1997
DOI:10.1080/00032719708004042
出版商: Taylor & Francis Group
关键词: stopped-flow;spectrophotometry;catecholamines;aminochrome
数据来源: Taylor
摘要:
A stopped flow method for the determination of dopamine and methyldopa is proposed. The method is based on the aerial oxidation of these catecholamines in strong alkali medium. The method was optimized using a spectrophotometer (λ = 360 nm) as detector. Calibration graphs were linear up to 2 × 10−4mol/L for dopamine and 3.0 × 10−4mol/L for methyldopa with quantification limits of 3.5 × 10−6mol/L and 4.3 × 10−7mol/L for dopamine and methyldopa, respectively. The method was successfully applied to the determination of catecholamines in pharmaceutical formulations.
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