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A Method for Sealing &bgr;‐Magnesia Windows into Steel Spectroscopic Absorption Furnaces and a Needle Valve for Controlling the Evacuation of Such Furnaces

 

作者: R. T. Brice,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1937)
卷期: Volume 8, issue 6  

页码: 209-212

 

ISSN:0034-6748

 

年代: 1937

 

DOI:10.1063/1.1752289

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A method is described whereby &bgr;‐magnesia windows may be sealed into heavy steel tubes, thus making them suitable for vacuum furnaces. These seals, utilizing copper or aluminum bands around the edges of the windows, have been made and tested up to 587°C without leaking. A needle valve is designed which permits the opening or closing of an evacuation port in the side of a vacuum furnace at will. This valve operates at the temperature of the furnace and does not introduce a cold spot into the absorption chamber. It has been tested up to 587°C and holds well against pressure differences of one atmosphere. Being made of stainless steel, it is relatively inert and is free from oxidation scale.

 

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