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Analytical Resolution of 4-ARYL-1,2,3,4,5,6,7,8-Octahydroquinazoline-2-Thiones using a Cellulose Chiral Stationary Phase

 

作者: Selma Saraç,   Mine Yarým,   Mevlüt Ertan,  

 

期刊: Analytical Letters  （Taylor Available online 1999）
卷期: Volume 32, issue 6  

页码: 1245-1254

 

ISSN:0003-2719

 

年代: 1999

 

DOI:10.1080/00032719908542893

 

出版商: Taylor & Francis Group

 

关键词: 4-Aryl-1,2,3,4,5,6,7,8-octahydroquinazoline-2-thiones;HPLC;chiral separation;cellulose tris(4-methylbenzoate)

 

数据来源: Taylor

 

摘要:

Racemic 4-aryl-1,2,3,4,5,6,7,8-octahydroquinazoline-2-thiones were resolved into their enantiomers by HPLC on cellulose tris(4-methylbenzoate) coated on silica gel using ethanol:n-hexane (70:30) as a mobile phase. A convenient method for preparation of cellulose tris(4-methylbenzoate) chiral stationary phase was described and the enantiomers were characterized by some chromatographic data.

 

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