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Complete1H and13C NMR spectral assignment of some polynitropolycyclic cage molecules by 2D NMR spectroscopy

 

作者: T. Axenrod,   B. Liang,   P. R. Dave,  

 

期刊: Magnetic Resonance in Chemistry  （WILEY Available online 1991）
卷期: Volume 29, issue 1  

页码: 9-17

 

ISSN:0749-1581

 

年代: 1991

 

DOI:10.1002/mrc.1260290104

 

出版商: John Wiley&Sons, Ltd.

 

关键词: Polynitropolycyclic molecules;Aromatic solvent‐induced shifts;NOE difference spectra;2D long‐range13C–1H shift correlated spectra;Nitro‐substituted adamantanes;Nitro‐substituted pentacycloundecanes

 

数据来源: WILEY

 

摘要:

AbstractThe1H and13C NMR spectra of several saturated polynitropolycyclic molecules were unambiguously assigned using aromatic solvent‐induced shifts, NOE difference spectra,1H–1H COSY spectra and 2D13C–1H shift correlated spectra, optimized either for one‐bond or long‐range13C–1

 

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