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Programmed Electronic X‐Ray Automatic Diffractometer

 

作者: S. C. Abrahams,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1962)
卷期: Volume 33, issue 9  

页码: 973-977

 

ISSN:0034-6748

 

年代: 1962

 

DOI:10.1063/1.1718043

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A high‐speed, high‐reliability, automatic diffractometer based on equi‐inclination geometry is described. Precomputed instructions are supplied on punched paper tape. The Miller indices of each reflection are recorded, both counter and initial crystal angles are set and recorded, the diffracted intensities at the required angular intervals in a fixed counter‐moving crystal stepwise scan are measured, and the final crystal angle is recorded automatically, all on punched paper tape. Angles are set to 0.01°. The output tape is processed to give the resulting corrected structure amplitudes on a common scale.

 

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