Electromemical Sample Contamination from Aqueous V (III) Oxygen Scrubbers
作者:
PaulaM. Deano,
J.W. Robinson,
RobertJ. Gale,
期刊:
Analytical Letters
(Taylor Available online 1984)
卷期:
Volume 17,
issue 6
页码: 447-450
ISSN:0003-2719
年代: 1984
DOI:10.1080/00032718408065292
出版商: Taylor & Francis Group
关键词: Oxygen scrubbers;stripping voltammetry
数据来源: Taylor
摘要:
We recommend that attention be given to the possibility of sample contamination in trace level electrochemical experiments when classical aqueous oxygen scrubbers are used. Although fresh electrolyte or water pre-saturators can be used to minimize ion carryover by aerosol spray, mercury vapor is still present in the gas stream. Many electrochemists now use solid catalysts (such as BASF R3-11, Badische Anilin and Soda-Fabrik), and their use, or that of pre-purified gases, are recommended to avoid such problems with purge gases in trace electroanalyses.
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