Characterization of ferroelectric lead zirconate titanate films by scanning force microscopy
作者:
Genaro Zavala,
Janos H. Fendler,
Susan Trolier-McKinstry,
期刊:
Journal of Applied Physics
(AIP Available online 1997)
卷期:
Volume 81,
issue 11
页码: 7480-7491
ISSN:0021-8979
年代: 1997
DOI:10.1063/1.365350
出版商: AIP
数据来源: AIP
摘要:
Scanning force microscopy (SFM) has been used for the determination of friction, phase transformation, piezoelectric behavior (in the contact mode), polarization state, and dielectric constant (in the noncontact mode) of nanometer regions of lead zirconate titanate (PZT) films. The use of the SFM tip in the contact mode, to polarize different nanoregions of the PZT film and to apply an oscillating field thereon, led to effective piezoelectric coefficients and piezoelectric loops. The measured effective piezoelectric coefficient was shown to depend appreciably on both the tip contact force and the quality of the tip-to-film electrical contact. In the noncontact mode, application of an ac signal (with a frequency &ohgr;) across the tip—PZT film—electrode system produced an oscillation of the tip at frequencies &ohgr; (fundamental or first harmonic) and 2&ohgr; (second harmonic). The signals at &ohgr; and 2&ohgr; were related to the state of polarization and the dielectric constant of the PZT film, respectively. Analysis of the combined contact, noncontact and friction force microscopic data provided insight into the structure and into the dielectric, ferroelectric, and piezoelectric properties of distinct nanoregions of the PZT film. ©1997 American Institute of Physics.
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