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Crystal Chemical Analysis of a Possibility of Photochemical Transformations in Crystals of C-(4-Methoxy-1-Vinyl)-N-Phenyl and C-(4-Methoxy-1-Vinyl)-N-Bromphenyl Nitrons

 

作者: A.N. Utienyshev,   S.M. Aldoshin,  

 

期刊: Molecular Crystals and Liquid Crystals Science and Technology. Section A. Molecular Crystals and Liquid Crystals  （Taylor Available online 1995）
卷期: Volume 270, issue 1  

页码: 123-134

 

ISSN:1058-725X

 

年代: 1995

 

DOI:10.1080/10587259508031022

 

出版商: Taylor & Francis Group

 

关键词: Nitrons;photochemical transformations;crystal structure

 

数据来源: Taylor

 

摘要:

An X-ray single crystal study of C-(4-methoxy-1-vinyl)-N-phenyl nitron (1) and C-(4-methoxy-1-vinyl)-N-bromphenyl nitron (2) was undertaken. The main crystal data: (1): C16H15NO2,a= 8.402(5) Åb= 5.408(3) Å,c= 14.554(7)Å, β= 93.1 (2)°,dcal.= 1.273 g/cm3,Vcal.=660.3 (2)Å3, Z= 2, Sp.gr.Pc.M= 253.32: (2):C16H14NO2Br,a= 17.586(6)Å,b= 14.543(5)Å,c= 5.632(4)Å, α=89.8(2)°, β,=90.8(2)°, γ= 98.9(2)°,dcal.= 1.554g/cm3,Vcal.= 1423.0(2)Å,Z= 4, Sp. gr. P1,M= 332.21

 

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