Response surface modeling of high pressure chemical vapor deposited blanket tungsten
作者:
Thomas E. Clark,
Mei Chang,
Cissy Leung,
期刊:
Journal of Vacuum Science&Technology B: Microelectronics and Nanometer Structures Processing, Measurement, and Phenomena
(AIP Available online 1991)
卷期:
Volume 9,
issue 3
页码: 1478-1486
ISSN:1071-1023
年代: 1991
DOI:10.1116/1.585453
出版商: American Vacuum Society
关键词: TUNGSTEN;CHEMICAL VAPOR DEPOSITION;LOW PRESSURE;HIGH TEMPERATURE;ELECTRICAL PROPERTIES;STRESSES
数据来源: AIP
摘要:
Chemical vapor deposited (CVD) blanket tungsten has been studied at high pressure (80 Torr) in a single‐wafer cold wall reactor using response surface modeling methods. Deposition factors studied include temperature (430–490 °C), H2partial pressure (6–30 Torr), WF6partial pressure (1–2 Torr), and the gas inlet to wafer surface separation (200–600 mils). Quadratic models were generated for deposition rate, resistivity, sheet resistance uniformity, film stress, step coverage, reflectance, and WF6conversion. The models were examined for consistency with previously reported results for CVD tungsten films, and were used to construct contour plots that aided a deposition process optimization search for a plug application. Optimization requirements for step coverage and sheet resistanceRsuniformity resulted in significant constraints on the usable factor space, while requirements for deposition rate, resistivity, stress, WF6conversion, and reflectance were largely met throughout the original factor space. The resulting optimized factor space was found to be relatively large and offered additional opportunities for fine tuning of the process. Finally, data from replicated trials showed the high pressure CVD blanket tungsten process to be highly reproducible.
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