A rheometer to measure the viscoelastic properties of polymer melts at ultrasonic frequencies
作者:
V. Thomas,
A. J. Giacomin,
A. Wolfenden,
期刊:
Review of Scientific Instruments
(AIP Available online 1994)
卷期:
Volume 65,
issue 7
页码: 2395-2401
ISSN:0034-6748
年代: 1994
DOI:10.1063/1.1144693
出版商: AIP
数据来源: AIP
摘要:
A rheometer which uses a piezoelectric ultrasonic composite oscillator has been developed to measure the viscoelastic properties,G’(&ohgr;) andG‘(&ohgr;), of polymer melts at ultrasonic frequencies. The storage and loss moduli of an ethylene–tetrafluoroethylene copolymer melt were measured at six frequencies in the range 0.25×106–1.28×106rad/s (between 40 and 200 kHz nominal frequency) and at a temperature of 280 °C. This ultrasonic instrument operates at strain amplitudes ranging from about 10−8to 10−3and is therefore ideally suited for linear viscoelastic property measurements.
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