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A rheometer for the measurement of a high shear modulus covering more than seven decades of frequency below 50 kHz

 

作者: T. Christensen,   N. B. Olsen,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1995)
卷期: Volume 66, issue 10  

页码: 5019-5031

 

ISSN:0034-6748

 

年代: 1995

 

DOI:10.1063/1.1146126

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A new rheometer is described. It consists of a transducer unit supplied with an electric impedance analyzing unit. The transducer unit converts a mechanical impedance into an electrical impedance by the piezoelectric effect. A detailed quantitative analysis of the interaction between the sample and the transducer is given. The real and imaginary parts of the shear modulus of a viscoelastic sample can be found in the frequency range of 1 mHz–50 kHz, modulus range of 0.1 MPa–10 GPa, and the temperature range of 150–300 K. The sample volume is 0.3 cm3and the strain amplitude is exceedingly small. The small size of the transducer allows for good temperature control and equilibration. It has a simple construction based on inexpensive components. Results on the supercooled liquid 2‐metyl‐2,4‐pentandiol at the glass transition obtained by the method are included. ©1995 American Institute of Physics.

 

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