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Miniature Bomb Calorimeter for the Determination of Heats of Combustion of Samples of the Order of 50 mg Mass

 

作者: William S. McEwan,   Carl M. Anderson,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1955)
卷期: Volume 26, issue 3  

页码: 280-284

 

ISSN:0034-6748

 

年代: 1955

 

DOI:10.1063/1.1771277

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A new bomb calorimeter for the combustion of very small quantities of organic materials has been constructed. The use of a small sample size is particularly important when dealing with explosive materials which when used in larger quantities, may detonate enough to spatter material from the crucible or when using substances which are difficult to prepare and purify in larger amounts. This calorimeter has several unique design features including a light weight bomb, coaxial stirrer, and flame holding sample holder.

 

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