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Solid-State NMR and X-Ray Crystallography: Complementary Tools for Structure Determination

 

作者: MargaretC. Etter,   RebeccaC. Hoye,   GailM. Vojta,  

 

期刊: Crystallography Reviews  （Taylor Available online 1988）
卷期: Volume 1, issue 4  

页码: 281-333

 

ISSN:0889-311X

 

年代: 1988

 

DOI:10.1080/08893118808081683

 

出版商: Taylor & Francis Group

 

关键词: Conformational analysis;cross-polarization (CP);hydrogen bonds;magic-angle spinning (MAS);multinuclear NMR;nuclear magnetic resonance (NMR);solid-state NMR;structure determination;X-ray crystallography

 

数据来源: Taylor

 

摘要:

High-resolution solid-state nuclear magnetic resonance is an analytical tool complementary to X-ray crystallography and it provides useful structural information for studying molecular structures. As well as being a general review, this article treats topics of current interest, especially the application of carbon-13 cross-polarization magic-angle spinning (CP/MAS) techniques to a wide range of chemical substances. There are also sections on hydrogen-bonded structures and on NMR studies of nuclei other than carbon, such as hydrogen. aluminum, silicon, phosphorus and tin.

 

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