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SYNTHESIS OF ORGANIC DEUTERIUM COMPOUNDS: X. METHYL-d3IODIDE AND DEUTERIUM SUBSTITUTION PRODUCTS OF METHYL ACETATE

 

作者: B. Nolin,  

 

期刊: Canadian Journal of Chemistry  （NRC Available online 1954）
卷期: Volume 32, issue 1  

页码: 1-3

 

ISSN:0008-4042

 

年代: 1954

 

DOI:10.1139/v54-001

 

出版商: NRC Research Press

 

数据来源: NRC

 

摘要:

Methyl-d3bromide was easily converted by treatment with calcium iodide into methyl-d3iodide in 94% yield. The latter was reacted on the 50-millimole scale with silver acetate or silver acetate-d3to yield methyl-d3acetate or methyl-d3acetate-d3. Methyl iodide and silver acetate-d3gave methyl acetate-d3.

 

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