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Synthesis, X-ray structure determination, and formation of 3,4,5-trichloroguaiacol occu...
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Synthesis, X-ray structure determination, and formation of 3,4,5-trichloroguaiacol occurring in kraft pulp spent bleach liquors
作者:
K. Lindström,
F. Österberg,
期刊:
Canadian Journal of Chemistry
(NRC Available online 1980)
卷期:
Volume 58,
issue 8
页码: 815-822
ISSN:0008-4042
年代: 1980
DOI:10.1139/v80-127
出版商: NRC Research Press
数据来源: NRC
摘要:
3,4,5-Trichloroguaiacol, which is formed during bleaching of chemical pulp and shown to bioaccumulate in fish, has been synthesized. The structure of the compound has been determined by means of X-ray analysis. The values of the13C nmr chemical shifts and melting point differ from those previously reported. A reaction mechanism is suggested for the formation of 3,4,5- and 4,5,6-trichloroguaiacol.
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