Identification and quantification of calystegines, polyhydroxyl nortropane alkaloids
作者:
Birgit Dräger,
期刊:
Phytochemical Analysis
(WILEY Available online 1995)
卷期:
Volume 6,
issue 1
页码: 31-37
ISSN:0958-0344
年代: 1995
DOI:10.1002/pca.2800060105
出版商: John Wiley&Sons, Ltd.
关键词: Calystegines;polyhydroxy nortropane alkaloids;thin layer chromatography;gas chromatography;silylation;mass spectroscopy
数据来源: WILEY
摘要:
AbstractCalystegines are a new group of polyhydroxy nortropane alkaloids that have recently been isolated fromCalystegia sepium.Thin layer chromatography systems have been developed for preliminary screening for these compounds, whilst quantitative analysis has been achieved, following silylation, by gas chromatography (GC) with an internal standard. The reproducibility and accuracy of the quantification method have been examined. The identity of the calystegines was assessed by co‐chromatography with reference samples, by chemical ionization mass spectroscopy (CI‐MS) of isolated calystegines, and by GC‐MS. Cultured roots ofAtropa belladonnawere examined for calyste
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