AbstractA new type of loop‐gap resonator, which because of its topology is called a “sectorial resonator,” is described in considerable analytical detail. It was used for31P NMR of the livers of two human adult normal volunteers. An effective strategy for suppression of signals from surface tissue was developed. Depth selection was achieved using a separate excitation coil, permitting a reasonable degree of control of the shape of the sensitive region by adjustment of the dimensions of the excitation coil and of the type of pulse delivered. In addition a new principle for cancellation is described: the topology of the sectorial resonator leads to cancellation signals from tissue masses at the two openings of the structure. Using a phase‐altenated repeated 90° FID pulse sequence, good spectra were achieved in 2.5 min that are free from contamination by the phosphocreatine peak. © 1986 Academic P