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Defocusing for the Schulz Technique of Determining Preferred Orientation

 

作者: E. Tenckhoff,  

 

期刊: Journal of Applied Physics  (AIP Available online 1970)
卷期: Volume 41, issue 10  

页码: 3944-3948

 

ISSN:0021-8979

 

年代: 1970

 

DOI:10.1063/1.1658393

 

出版商: AIP

 

数据来源: AIP

 

摘要:

During measurement of preferred crystallographic orientation with the Schulz x‐ray diffraction technique, several factors can cause defocusing. Earlier investigations showed that tilt of the specimen in &PHgr;, the angle between the normal to the sample surface and the normal to the diffracting plane, is the most severe limitation for the Schulz reflection technique. The present study shows that this defocusing effect is strongly dependent on the size of the Bragg diffraction angle &thgr;: The greater the Bragg angle, the smaller the decrease in intensity for a given tilt angle of &PHgr;. On the other hand, the absorption coefficient &mgr; of the sample has no influence on the decrease in intensity with increasing tilt in &PHgr;, and its effect is negligibly small for most metals. Correction factors for the loss of intensity can be derived and have a general analytic form, but different coefficients are required for each goniometer setting.

 

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