Determination of Vitamin K1by Adsorptive Stripping Square-Wave Voltammetry
作者:
J.C. Vire,
V. Lopez,
G.J. Patriarche,
G.D. Christian,
期刊:
Analytical Letters
(Taylor Available online 1988)
卷期:
Volume 21,
issue 12
页码: 2217-2225
ISSN:0003-2719
年代: 1988
DOI:10.1080/00032718808059904
出版商: Taylor & Francis Group
关键词: Vitamin K1;;adsorptive stripping;square-wave voltammetry;differential pulse voltammetry
数据来源: Taylor
摘要:
The adsorption of vitamin Ki at a hanging mercury drop electrode at pH 4.2 allows the determination of this compound in the 1 × 10−6M−1 × 10−9Mconcentration range. Applying a square-wave potential scan provides a 200-fold increase of the peak current compared to differential pulse stripping voltammetry. The influence of several operational parameters such as the nature and the pH of the supporting electrolyte, the deposition time and the potential are discussed. Interactions between the adsorbed molecules occur during the deposition step.
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