Determination of Norfloxacin by the Means of Oscillopolarographic Titration
作者:
W. Xiuling,
Z. Shumin,
Z. Wenwei,
C. Qihua,
期刊:
Analytical Letters
(Taylor Available online 1996)
卷期:
Volume 29,
issue 1
页码: 131-139
ISSN:0003-2719
年代: 1996
DOI:10.1080/00032719608000397
出版商: Taylor & Francis Group
关键词: oscillopolarographic titration;norfloxacin;sodium tetraphenylboron;thallous sulfate
数据来源: Taylor
摘要:
An oscillopolarographic titration method for the determination of norfloxacin in materials and capsules is described in this paper. The norfloxacin is precipitated as NOR-TPB. Filtrates were titrated with thallous sulfate in an alkaline solution. The recoveries ranged from 99.10% to 100.53% by the use of a standard addition. Experiments showed that the proposed method gave the same results as the approach using nonaqueous titration as USP and CSP.
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