Magnetic properties and microstructure studies of Sm–Fe magnetic thin films
作者:
H. Sun,
T. Tomida,
S. Hirosawa,
期刊:
Journal of Applied Physics
(AIP Available online 1997)
卷期:
Volume 81,
issue 1
页码: 328-334
ISSN:0021-8979
年代: 1997
DOI:10.1063/1.364114
出版商: AIP
数据来源: AIP
摘要:
Binary SmxFe100−x(2<x<12) thin films were made by rf sputtering of the target onto preheated quartz glass substrates. Structural characterization, magnetic measurement, and microstructure observation were carried out by x-ray diffractometer, vibrating sample magnetometer, scanning electron microscope, and transmission electron microscope (TEM), respectively. Directly crystallized films were synthesized at substrate temperature higher than 400 °C and the main phase of the films is the ThMn12-type tetragonal phase with lattice parametersa=8.65 Å andc=4.78 Å. Films have the predominant [111] and [001] crystallographic texture when the substrate temperature is lower and higher than 600 °C, respectively. The perpendicular magnetization measured under the applied field of 22 kOe is about 30&percent; higher than the saturation magnetization of bulk SmFe11Ti. Coercivities of about 4.0 kOe can be obtained in the substrate temperature range between 430 and 550 °C with grain size of 0.2–0.3 &mgr;m. Cross-sectional TEM microstructure observations show significant columnar structures in the films. The [001] texture formed in the films is also clearly reflected by the planar and cross-sectional TEM diffraction patterns. ©1997 American Institute of Physics.
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